Introduction:
Flame test is an experiment used to identify/distinguish
metals using colors exposed to a flame.
Since metallic halides easily
evaporate, the test is usually done using the halide components of metals. Out
of the halides, chlorides are frequently used because chlorides give a fast
change of color when exposed to the flame as opposed to other halides.
Materials needed:
·
A rod of platinum, nichrome, asbestos or
graphite
·
Concentrated HCl solution
·
Bunsen burner
·
Metallic salt (a chloride of a metal)
·
A cobalt glass (if necessary)
Method:
- Insert the rod of platinum, nichrome, asbestos or graphite into a concentrated solution of HCl.
- Hold the rod to a Bunsen flame. (to the colorless region)
- Continue this experiment until the top region of the flame turns colorless.
- Form a pulp by mixing the metallic salt with the concentrated HCl solution and apply the pulp to the rod.
- Finally, hold the rod to the Bunsen flame and observe the color changes.
Observations:
Note:
Ø
If Sodium (Na) is present in minute quantities,
the yellow color may be observed as flashes.
Ø
Sometimes, the purple color may not be observed
for Potassium (K) during the test due to the presence of impurities. However,
this problem can be minimized if a cobalt glass is used (cobalt absorbs all
colors except Potassium (K).
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